Estrogens, Estradiol, Ethinylestradiol

This article compares the extraction of steroidal estrogens from tap water by using two extractions method, Liquid – Liquid Extraction and SPE with AFFINIMIP®SPE Estrogens prior analysis with GC-MS/MS and GC-HRMS. For SPE, recovery yields between 99 and 113% were obtained.

Determination of steroidal oestrogens in tap water samples using solid-phase extraction on a molecularly imprinted polymer sorbent and quantification with gas chromatography-mass spectrometry (GC-MS), D. Zacs, I. Perkons, V. Bartkevics, Environ Monit Assess 188, 433, 2016.

Please note the article using AFFINIMIP®SPE Phenolics for the determination of ultra trace levels of 13 estrogenic EDCs by UHPLC-MS/MS

13 analytes: estrone (E1), 17α-estradiol (α-E2), 17β-estradiol (β-E2), estriol (E3), 17α-ethinylestradiol (EE2), diethylstilbestrol (DES), bisphenol A (BPA), bisphenol S (BPS), 4-n-octylphenol (OP), 4-n-nonylphenol (NP), coumestrol (COU), genistein (GEN), and enterolactone (ENT).

Development of a molecular recognition based approach for multi-residue extraction of estrogenic endocrine disruptors from biological fluids coupled to liquid chromatography-tandem mass spectrometry measurement, R. Bousoumah, J. P. Antignac, V. Camel, M. Grimaldi, P. Balaguer, F. Courant, E. Bichon, M.-L. Morvan, B. Le Bizec, Anal Bioanal Chem, 407: 8713, 2015.

Unraveling estradiol metabolism and involvement in the reproductive cycle of non-vertebrate animals: the sea urchin model. S. Mercurio, P. Tremolada, M. Nobile, D. Fernandes, C. Porte, M. Sugni, Steroids, vol. 104, 25-36, 2015.

On-line molecularly imprinted solid-phase extraction coupled to liquid chromatography-tandem mass spectrometry for the determination of hormones in water and sediment samples, D. Matějíček, J. Vlček, A. Burešová, P. Pelcová, J. Sep. Sci., 36 (9-10), 1509-1515, 2013.

The use of molecularly imprinted polymers for the multicomponent determination of endocrine-disrupting compounds in water and sediment, D. Matějíček, A. Grycová, J. Vlček, J. Sep. Sci., 36(6), 1097-1103, 2013.

Molecularly imprinted polymer applied to the selective isolation of urinary steroid hormones: An efficient tool in the control of natural steroid hormones abuse in cattle, M. Doué, E. Bichon, G. Dervilly-Pinel, V. Pichon, F. Chapuis-Hugon, E. Lesellier, C. West, F. Monteau, B. Le Bizec, J. Chrom A, 1270, 51-56, 2012.

Solid-phase extraction using molecularly imprinted polymer for selective extraction of natural and synthetic estrogens from aqueous samples, P. Lucci, O. Núñez, M.T. Galceran, J. Chrom. A, 1218,(30), 4828-4833, 2011.

Quantification of estrogens at ppt levels in bovine plasma by AFFINIMIP® SPE and GC-MS/MS analysis, S. Rochereau, E. Bichon, F. Courant, F. Monteau, S. Prévost, F. Hanganu, N. Cesbron, G. Dervilly-Pinel, B. Le Bizec.

This poster was presented at Euroresidues VIIth conference, Egmond aan Zee, The Nertherlands, 14th-16th May 2012 by the French reference laboratory on residues and contaminants in food (LABERCA – ONIRIS).

Original method for analysis of Estrogens and Bisphenol A, Endocrine Disrupting Chemicals using solid phase extraction based on molecularly imprinted polymer, D.Derrien, M. Mulet, B. Chevalier, F. Alix, C.Pérollier, O.Lépine, K.Naraghi* , Johann Travers, S. Bayoudh, présenté à ISEAC-37 at Antwerp, Belgium, May 22nd, 2012.

High efficiency of semi-preparative Supercritical Fluid Chromatography with Molecularly Imprinted Polymer as stationary phase (SFC-MIP). Application on urinary steroids purification for IRMS analysis, M. DOUE, E. BICHON, F. MONTEAU, B. LE BIZEC.

Poster presented at the 2nd International Symposium on HTSP , Brugge, Belgium, 31st January – 3rd February 2012 by the French reference laboratory on residues and contaminants in food (LABERCA – ONIRIS).

How to improve analytical strategies to monitor growth promoting agents misuse in cattle, E. Bichon, S. Rochereau, L. Sérée, S. Prevost, F. Monteau, B. Le Bizec.

This conference was presented at 5th international Symposium on Recent Advances in Food Analysis (RAFA), Prague, Czech Republic, 1-4 November 2011 by the French reference laboratory on residues and contaminants in food (LABERCA – ONIRIS).

New method for extraction of Estrogens On Molecularly Imprinted Polymer, D. Derrien, C. Pérollier, O. Lépine, S. Bayoudh, K. Naraghi presented at PITTCON2011, Atlanta, Georgia, March 13 – 18, 2011.